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Aurora AI 1200 Graphite Furnace Atomic Absorption Spectrophotometer

The AI 1200 Atomic Absorption Spectrometer's graphite furnace reduces and even eliminates many of the problems that are normally associated with GFAAS. These include; memory effects, poor atomisation efficiency, slow analysis and high background. How is this accomplished?

Transverse Heating

Spatially isothermal atomisation is critical to achieving accurate analysis with GFAAS. Non-isothermal conditions cause memory effects, increased background and poor atomisation efficiency.

Aurora AI 1200 Isothermal Conditions

This is why the AI 1200 uses a transversely heated graphite furnace. In contrast to longitudinally-heated graphite furnaces, which create temperature gradients within the graphite tube, Aurora Instruments' transversely heated furnace provides near isothermal atomisation conditions.

The graph shown above demonstrates the spatially isothermal temperature profile of the AI 1200's transversely heated graphite furnace.

High Heating Rate

Temporally isothermal atomisation is the ideal condition for atomisation in GFAAS. In the AI 1200 this is achieved by using an industry leading 3800 K/s heating rate, which results in the sample being atomised when the temperature of the furnace is stable. The AI 1200 GF provides programming flexibility.

  • Heating programs of up to 30 individual steps.
  • Ramp time can be varied in steps of 0.1 second.
  • Hold time is selectable from 0 seconds up to 99 seconds in steps of 0.1 second.

Superior Temperature Control

The most important stage affecting the reproducibility of graphite atomisation is the drying stage. If the temperature control of the furnace is inaccurate, then reproducible drying conditions may be impossible to achieve. As this is the case, Aurora have focused their efforts on making this stage of the process easy for the chemist.

The AI 1200 uses a specially designed temperature sensor for the temperatures in the low temperature range in addition to the high temperature sensors already found in previous models. This sensor has its own calibration program that results in a temperature control that is accurate to within 1 degree celsius. This provides actual objective data, unlike competitive instruments, because the Aurora system does not use simulated logrithms.

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